You will need to enter into a separation agreement to make the agreed upon terms binding and enforceable. You will want to include that the marital residence is to become your sole and separate property and that your husband shall cooperate as needed in order for you to refinance (i.e. sign a deed, sign a free trader agreement, etc.).
In conjunction with the separation agreement, go ahead and reach out to mortgage lenders about their requirements to refinance. Oftentimes your husband can sign the deed and free trader contemporaneously with the refinance rather than before. Don’t get an appraisal done until you have direction from your lender about when to have that done.
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